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Synthesis and crystal structure of NZP-type thorium-zirconium phosphate

Autor(es) y otros:
Orlova, Albina I.; Volgutov, Valeriy Yu; Castro Castro, Germán Rafael; García-Granda, SantiagoAutoridad Uniovi; Khaynakov, SergiyAutoridad Uniovi; García Menéndez, José RubénAutoridad Uniovi
Fecha de publicación:
2009
Versión del editor:
http://dx.doi.org/10.1021/ic9013812
Citación:
Inorganic Chemistry, 48 (19), p. 9046-9047 (2009); doi:10.1021/ic9013812
Descripción física:
p. 9046-9047
Resumen:

Microcrystals of Th1/4Zr2(PO4)3 were synthesized by thermal treatment (900 °C) of the material obtained using sol−gel technology (including organic complex formation and etherification). Their structure [hexagonal, P3̅c, a = b = 8.7311(4) Å, c = 23.309(2) Å] includes the three-dimensional [Zr2(PO4)3]− NASICON-type network and extraframework 6-fold-coordinated thorium(IV) cations.

Microcrystals of Th1/4Zr2(PO4)3 were synthesized by thermal treatment (900 °C) of the material obtained using sol−gel technology (including organic complex formation and etherification). Their structure [hexagonal, P3̅c, a = b = 8.7311(4) Å, c = 23.309(2) Å] includes the three-dimensional [Zr2(PO4)3]− NASICON-type network and extraframework 6-fold-coordinated thorium(IV) cations.

URI:
http://hdl.handle.net/10651/8296
ISSN:
0020-1669
Identificador local:

20090236

DOI:
10.1021/ic9013812
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