Repositorio Institucional de la Universidad de Oviedo

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This work used samples provided by the Integrated Ocean Drilling Program (IODP). The IODP is sponsored by the U.S. National Science Foundation and participating countries under management of the Joint Oceanographic Institutions (JOI), Inc. We thank the shipboard party of IODP Expeditions 303 and 306 and A. Wuelbers and W. Hale for their help during sampling at Bremen Core Repository. We are grateful to Mike Bolshaw, Dave Spanner, and Tom Hindson for help in the laboratory and Eelco Rohling and Heiko Pälike for useful dis- cussions. Financial support was provided by the Natural Environmental Research Council, NERC, in the form of a Ph.D. studentship to C.T.B. (ref- erence NER/S/A/2006/14218) and a UK IODP grant to P.A.W., R.S., and I.B. I.B. is grateful to UK IODP for financial support for shipboard and postcruise participation in IODP Expedition 306. This study was also partly funded by the European Commission while O.F. held a Marie Curie IntraEuropean Fellowship at the University of Southampton (project PLIO‐CLIMATE). We thank Tom Cronin and an anonymous reviewer for comments and suggestions that significantly improved the manuscript