Data Documentation for the supplemetary material of the article "Photochemical carboborylation and three-component difunctionalization of a,b-unsaturated ketones with boronic acids via tosylhydrazones". Chemical Science, doi: 10.1039/d4sc06537a 
 

General Information
Supplementary information for the article "Photochemical carboborylation and three- component difunctionalization of a,b-unsaturated ketones with boronic acids via tosylhydrazones" Chemical Science: DOI: 10.1039/d4sc06537a. The data are contained in a word .docx file with the chemdraw and NMR data embebed. NMR data in mestrenova format can be retrieved from the file. A zip file containing all the NMR data is also provided.

Name of dataset: 
SupportingCS-2024-19626

Name of data files in data set:
SupportingCS-2024-19626
NMR-CS-2024-19626.zip

Dataset language:
English

Date the data set was last modified:
25-10-2024 

Funder:
Financial support of this work by Ministerio de Ciencia e
Innovaci´on of Spain (Agencia Estatal de Investigaci´on: grant
MCINN-23-PID2022-140635NB-I00 ?nanced by MCIN/AEI/
10.13039/501100011033/FEDER, UE). A FPI predoctoral contract
to ´A.V.-M. (MCINN-24-PREP2022-000214) and a “Ram´on y Cajal”
postdoctoral grant to M. P. (MCINN-24-RYC2022-035485-I) by
Ministerio de Ciencia e Innovaci´on of Spain (Agencia Estatal de
Investigaci´on) are gratefully acknowledged.

How to cite data:
Valdés-Maqueda, Á.; Plaza, M.; Valdés, C. Photochemical Carboborylation and Three-Component Difunctionalization of a,ß-Unsaturated Ketones with Boronic Acids via Tosylhydrazones. Chem. Sci. 2024, 15 (46), 19626–19633. https://doi.org/10.1039/D4SC06537A.]

Methodology for data collection: 


Data collector(s): 
Alvaro Valdés-Maqueda, Manuel Plaza

Date of data collection: 
2023

Person to contact with questions: 

Carlos Valdés

Data entry:
12-05-2025

Software (including version #) used to prepare data set: 
MSword, Chemdraw22.2, MestreNova 14


Data processing that was performed: 
NMR FIDs were processed with MestreNova, copied and pasted in the Word document


Variables


File Overview
SupportingCS-2024-19626: a .docx file containing all the experimental and NMR data,: NMR mestrenova files can be retrieved oorm the document.
NMR-CS-2024-19626.zip: a zip file containing the NMR data. There is one folder for each compound named with the numbers of the publication. Each folder contains independent folders for the 1H NMR data (1) and the 13C NMR data (2).